Structures by: Macdonald C. L.
Total: 192
C37H21ClF12N5Sn,Cl3Sn
C37H21ClF12N5Sn,Cl3Sn
Dalton transactions (Cambridge, England : 2003) (2019) 48, 22 7835-7843
a=9.1861(13)Å b=13.4274(18)Å c=17.478(2)Å
α=75.357(4)° β=80.979(4)° γ=79.243(4)°
C35H25F6N5O6S2Sn
C35H25F6N5O6S2Sn
Dalton transactions (Cambridge, England : 2003) (2019) 48, 22 7835-7843
a=14.776(11)Å b=12.477(11)Å c=20.178(16)Å
α=90° β=111.21(2)° γ=90°
C19H11ClGeN3O2,Cl3Ge
C19H11ClGeN3O2,Cl3Ge
Dalton transactions (Cambridge, England : 2003) (2019) 48, 22 7835-7843
a=10.4493(7)Å b=12.5471(7)Å c=16.9264(10)Å
α=90° β=96.429(2)° γ=90°
C33H25ClGeN5,CF3O3S
C33H25ClGeN5,CF3O3S
Dalton transactions (Cambridge, England : 2003) (2019) 48, 22 7835-7843
a=8.9152(4)Å b=13.6048(6)Å c=14.3903(7)Å
α=117.3640(10)° β=95.9400(10)° γ=90.1870(10)°
C25H21ClGeN5,Cl3Ge
C25H21ClGeN5,Cl3Ge
Dalton transactions (Cambridge, England : 2003) (2019) 48, 22 7835-7843
a=10.4681(7)Å b=16.4860(9)Å c=15.2025(9)Å
α=90° β=94.718(2)° γ=90°
2(Cl3Sn),C66H50N10Ni,0.5(C4H8O),C4H5O
2(Cl3Sn),C66H50N10Ni,0.5(C4H8O),C4H5O
Dalton transactions (Cambridge, England : 2003) (2019) 48, 22 7835-7843
a=13.7350(7)Å b=14.0932(8)Å c=19.9403(12)Å
α=82.180(2)° β=76.134(2)° γ=63.862(2)°
C16H16O4P2S4
C16H16O4P2S4
Dalton Trans. (2017)
a=11.6592(5)Å b=8.9815(4)Å c=10.3322(5)Å
α=90° β=115.786(2)° γ=90°
C24H24O6P2S6,2(CH2Cl2)
C24H24O6P2S6,2(CH2Cl2)
Dalton Trans. (2017)
a=10.0951(3)Å b=25.1596(8)Å c=14.0295(4)Å
α=90° β=103.6580(10)° γ=90°
C42H54O15P2S6
C42H54O15P2S6
Dalton Trans. (2017)
a=8.3950(13)Å b=14.979(2)Å c=19.671(3)Å
α=85.760(6)° β=78.209(5)° γ=74.703(6)°
C33H36BN2O2P
C33H36BN2O2P
Dalton Trans. (2017)
a=9.6725(4)Å b=11.3305(4)Å c=14.4827(6)Å
α=101.512(2)° β=100.403(2)° γ=101.893(2)°
C25H36BN2O2P
C25H36BN2O2P
Dalton Trans. (2017)
a=10.7605(4)Å b=11.2811(4)Å c=12.5055(4)Å
α=111.6550(10)° β=98.380(2)° γ=110.8890(10)°
C21H27BNO3P
C21H27BNO3P
Dalton Trans. (2017)
a=6.2343(10)Å b=9.4532(13)Å c=17.992(3)Å
α=86.725(5)° β=89.957(6)° γ=84.737(5)°
C23H31BNO3P
C23H31BNO3P
Dalton Trans. (2017)
a=9.5854(7)Å b=9.7989(8)Å c=15.9177(14)Å
α=75.187(3)° β=80.891(3)° γ=63.041(3)°
C23H31BNO2PS
C23H31BNO2PS
Dalton Trans. (2017)
a=10.3603(12)Å b=17.1280(19)Å c=26.966(3)Å
α=92.761(4)° β=93.308(4)° γ=90.282(4)°
Indium(I) trifluoromethanesulfonate
[In][CF3O3S]
Chemical communications (Cambridge, England) (2004) 2 250-251
a=4.8934(4)Å b=7.2298(6)Å c=16.9499(15)Å
α=91.011(2)° β=93.835(2)° γ=101.711(2)°
Triphosphenium iodide
[C26H24P3][I1]
Chemical Communications (Cambridge, United Kingdom) (2003) 15 1946-1947
a=10.1340(5)Å b=13.5928(7)Å c=19.7256(10)Å
α=71.9900(10)° β=81.3070(10)° γ=68.8530(10)°
Triphosphenium tetraphenylborate
[C26H24P3][C24H20B]
Chemical Communications (Cambridge, United Kingdom) (2003) 15 1946-1947
a=11.9875(6)Å b=17.5408(6)Å c=20.9570(9)Å
α=90.00° β=113.179(15)° γ=90.00°
(CGC)antimony chloride
C15H27ClNSbSi
Chemical Communications (Cambridge, United Kingdom) (2003) 3 430-431
a=8.146(5)Å b=24.618(5)Å c=8.984(5)Å
α=90.000(5)° β=95.488(5)° γ=90.000(5)°
C13H3F10Ga
C13H3F10Ga
Chemical Communications (Cambridge, United Kingdom) (2003) 3 424-425
a=13.979(5)Å b=6.507(5)Å c=15.782(5)Å
α=90.000(5)° β=114.748(5)° γ=90.000(5)°
C8H6AlF5
C8H6AlF5
Chemical Communications (Cambridge, United Kingdom) (2003) 3 424-425
a=7.1912(14)Å b=7.4838(15)Å c=18.436(4)Å
α=84.47(3)° β=88.73(3)° γ=64.68(3)°
(CGC)phosphium aluminum tetrachloride
[C15H27NPSi][AlCl4]
Chemical Communications (Cambridge, United Kingdom) (2003) 3 430-431
a=18.064(4)Å b=8.3447(17)Å c=30.103(6)Å
α=90.00° β=90.00° γ=90.00°
(CGC)arsenic chloride
C15H27ClNASSi
Chemical Communications (Cambridge, United Kingdom) (2003) 3 430-431
a=6.953(5)Å b=17.258(5)Å c=14.991(5)Å
α=90.000(5)° β=91.669(5)° γ=90.000(5)°
(CGC)phosphorous chloride
C15H27ClNPSi
Chemical Communications (Cambridge, United Kingdom) (2003) 3 430-431
a=14.969(5)Å b=15.300(5)Å c=15.506(5)Å
α=90.000(5)° β=90.000(5)° γ=90.000(5)°
(CGC)phosphium arsenium tetrachloride
[C15H27NAsSi][AlCl4]
Chemical Communications (Cambridge, United Kingdom) (2003) 3 430-431
a=18.184(4)Å b=8.2774(17)Å c=30.284(6)Å
α=90.00° β=90.00° γ=90.00°
Securinine
C13H15NO2
Chemical communications (Cambridge, England) (2009) 34, 4 463-465
a=6.9876(10)Å b=9.3485(13)Å c=16.411(2)Å
α=90.00° β=90.00° γ=90.00°
C10H15NO
C10H15NO
Chemical communications (Cambridge, England) (2009) 34, 4 463-465
a=7.4042(10)Å b=8.5718(11)Å c=14.7778(19)Å
α=90.00° β=90.00° γ=90.00°
C24H32Cl1Cu1N2
C24H32Cl1Cu1N2
Chemical communications (Cambridge, England) (2008) 46 6200-6202
a=9.3700(17)Å b=9.4399(17)Å c=14.913(3)Å
α=81.078(2)° β=85.418(2)° γ=64.894(2)°
C7H12NS,I
C7H12NS,I
Dalton transactions (Cambridge, England : 2003) (2016) 45, 5 2138-2147
a=7.2083(10)Å b=8.0237(11)Å c=8.8800(12)Å
α=78.7720(10)° β=82.5190(10)° γ=73.7020(10)°
C8H14NS,I
C8H14NS,I
Dalton transactions (Cambridge, England : 2003) (2016) 45, 5 2138-2147
a=12.0281(14)Å b=7.7753(9)Å c=11.5619(13)Å
α=90° β=90° γ=90°
C11H14NS,I
C11H14NS,I
Dalton transactions (Cambridge, England : 2003) (2016) 45, 5 2138-2147
a=17.471(3)Å b=13.112(2)Å c=5.2955(9)Å
α=90° β=90° γ=90°
C18H18N2S2
C18H18N2S2
Dalton transactions (Cambridge, England : 2003) (2016) 45, 5 2138-2147
a=8.4609(10)Å b=9.3845(11)Å c=20.267(2)Å
α=90° β=90° γ=90°
C14H22N2PS2,I
C14H22N2PS2,I
Dalton transactions (Cambridge, England : 2003) (2016) 45, 5 2138-2147
a=14.6665(7)Å b=10.2797(5)Å c=13.4062(7)Å
α=90° β=118.4096(18)° γ=90°
C41H32P4S
C41H32P4S
Dalton transactions (Cambridge, England : 2003) (2016) 45, 14 6251-6258
a=8.9112(2)Å b=14.6975(4)Å c=26.2859(6)Å
α=90° β=98.2890(10)° γ=90°
C41H32AuClP4
C41H32AuClP4
Dalton transactions (Cambridge, England : 2003) (2016) 45, 14 6251-6258
a=13.5468(5)Å b=16.8119(5)Å c=16.3995(6)Å
α=90° β=106.8580(10)° γ=90°
[(dppe)P 1+]2 [SnCl6 2-] . 2 CH2Cl2
2C26H24P3,Cl6Sn2,2CH2Cl2
Acta Crystallographica Section E (2006) 62, 6 m1235-m1236
a=10.8589(4)Å b=11.5303(5)Å c=13.0841(5)Å
α=68.7770(10)° β=79.7740(10)° γ=81.3320(10)°
[(Ph3P)2P +] [AlCl4 -] . 0.5 CH2Cl2
C36H30P3,Cl4Al,0.5CH2Cl2
Acta Crystallographica Section E (2006) 62, 8 m1869-m1870
a=33.283(5)Å b=9.2443(13)Å c=23.979(4)Å
α=90.00° β=90.00° γ=90.00°
Cobaltocenium triflate
C10H10Co,CF3O3S
Acta Crystallographica Section E (2005) 61, 10 m2103-m2105
a=16.326(3)Å b=13.119(3)Å c=17.644(3)Å
α=90.00° β=106.069(2)° γ=90.00°
[18]crown-6 adduct of dimethylindium trifluoromethanesulfonate
C14H30InO6,CF3O3S
Acta Crystallographica Section E (2011) 67, 2 m233-m234
a=12.9580(19)Å b=12.7242(19)Å c=14.683(2)Å
α=90.00° β=112.801(2)° γ=90.00°
1,1,1-Tris(dimethylamino)-2-[tris(dimethylamino)phosphoranylidene]diphosphinium tetraphenylborate tetrahydrofuran monosolvate
C12H36N6P3,C24H20B,C4H8O
Acta Crystallographica Section E (2014) 70, 6 o691
a=13.0859(17)Å b=11.8258(16)Å c=27.504(4)Å
α=90° β=98.930(2)° γ=90°
C4H12I3PPb
C4H12I3PPb
ACS omega (2018) 3, 12 17077-17082
a=10.0382(8)Å b=10.0382(8)Å c=23.738(2)Å
α=90° β=90° γ=120°
C4H12P,I
C4H12P,I
ACS omega (2018) 3, 12 17077-17082
a=8.1978(10)Å b=8.1978(10)Å c=6.0037(8)Å
α=90° β=90° γ=90°
C8H22P2,2(PbI3)
C8H22P2,2(PbI3)
ACS omega (2018) 3, 12 17077-17082
a=15.3593(6)Å b=11.1506(4)Å c=7.9441(3)Å
α=90° β=100.8890(10)° γ=90°
C19H18P,2I3Pb,0.5(C2H3N)
C19H18P,2I3Pb,0.5(C2H3N)
ACS omega (2018) 3, 12 17077-17082
a=24.560(2)Å b=13.0686(11)Å c=16.1499(14)Å
α=90° β=110.037(2)° γ=90°
C12H28P,PbI3
C12H28P,PbI3
ACS omega (2018) 3, 12 17077-17082
a=16.0770(7)Å b=16.3313(9)Å c=16.9952(9)Å
α=90° β=107.066(2)° γ=90°
C30H28BrN2P
C30H28BrN2P
Organometallics (2009) 28, 15 4377
a=11.4785(12)Å b=17.6796(18)Å c=37.784(4)Å
α=90.00° β=93.030(2)° γ=90.00°
C22H28N2P,I3
C22H28N2P,I3
Organometallics (2009) 28, 15 4377
a=14.0085(14)Å b=15.5780(16)Å c=24.014(2)Å
α=90.00° β=90.00° γ=90.00°
C26H24P31,I1
C26H24P31,I1
Inorganic Chemistry (2006) 45, 17 6864-6874
a=10.1179(13)Å b=13.5649(17)Å c=19.688(3)Å
α=71.9700(10)° β=81.2800(10)° γ=68.8660(10)°
C27H26P31,I1
C27H26P31,I1
Inorganic Chemistry (2006) 45, 17 6864-6874
a=10.9315(10)Å b=19.2143(18)Å c=12.9085(12)Å
α=90.00° β=110.931(2)° γ=90.00°
C27H26P31,C24H20B1
C27H26P31,C24H20B1
Inorganic Chemistry (2006) 45, 17 6864-6874
a=12.244(3)Å b=17.883(3)Å c=21.258(4)Å
α=90.00° β=114.957(10)° γ=90.00°
C27H26P31,CF3O3S1,CH2Cl2
C27H26P31,CF3O3S1,CH2Cl2
Inorganic Chemistry (2006) 45, 17 6864-6874
a=9.303(3)Å b=15.661(5)Å c=11.127(3)Å
α=90.00° β=109.605(3)° γ=90.00°
C27H26P31,Cl4Ga1
C27H26P31,Cl4Ga1
Inorganic Chemistry (2006) 45, 17 6864-6874
a=9.7274(16)Å b=14.815(3)Å c=21.255(3)Å
α=90.00° β=106.894(6)° γ=90.00°
C27H261,F6P41
C27H261,F6P41
Inorganic Chemistry (2006) 45, 17 6864-6874
a=12.690(8)Å b=15.736(9)Å c=17.815(8)Å
α=90.00° β=131.57(3)° γ=90.00°
C27H26P31,B0.26F1.03I0.741
C27H26P31,B0.26F1.03I0.741
Inorganic Chemistry (2006) 45, 17 6864-6874
a=12.741(5)Å b=15.580(5)Å c=17.640(5)Å
α=90.00° β=133.479(17)° γ=90.00°
Bis(diphenylphosphino)ethane tetraiodine adduct
C26H24I4P2
Inorganic Chemistry (2006) 45, 17 6864-6874
a=15.2158(8)Å b=15.2876(8)Å c=12.3342(6)Å
α=90.00° β=90.00° γ=90.00°
4(C33H25ClGeN5),4(Cl3Ge),CH2Cl2
4(C33H25ClGeN5),4(Cl3Ge),CH2Cl2
Dalton transactions (Cambridge, England : 2003) (2019) 48, 22 7835-7843
a=14.1393(9)Å b=15.1768(9)Å c=16.3072(11)Å
α=86.094(2)° β=74.051(2)° γ=76.567(2)°
(CGC)phosphium stibocenium tetrachloride
[C15H27NSbSi][AlCl4]
Chemical Communications (Cambridge, United Kingdom) (2003) 3 430-431
a=10.064(5)Å b=11.154(5)Å c=12.120(5)Å
α=92.411(5)° β=114.403(5)° γ=110.722(5)°
C6H10NS,I
C6H10NS,I
Dalton transactions (Cambridge, England : 2003) (2016) 45, 5 2138-2147
a=8.5748(2)Å b=7.6434(2)Å c=13.3454(3)Å
α=90° β=92.1710(10)° γ=90°
C41H32P4
C41H32P4
Dalton transactions (Cambridge, England : 2003) (2016) 45, 14 6251-6258
a=9.0357(4)Å b=14.2215(5)Å c=26.5604(12)Å
α=90° β=98.960(2)° γ=90°
C26H24P31,C24H20B1
C26H24P31,C24H20B1
Inorganic Chemistry (2006) 45, 17 6864-6874
a=12.0031(8)Å b=17.5742(12)Å c=19.6302(13)Å
α=90.00° β=100.8930(10)° γ=90.00°
C22H28N4P,Br,0.36(C2H3N)
C22H28N4P,Br,0.36(C2H3N)
Inorganic chemistry (2016) 55, 14 7152-7166
a=12.5586(9)Å b=14.5318(13)Å c=12.9162(12)Å
α=90° β=94.823(3)° γ=90°
C18H21N4P,2(CF3O3S),C2H3N
C18H21N4P,2(CF3O3S),C2H3N
Inorganic chemistry (2016) 55, 14 7152-7166
a=8.0203(4)Å b=13.8070(6)Å c=13.9727(6)Å
α=103.508(2)° β=105.014(2)° γ=98.757(2)°
C26H36N4P,C2H3N,Br
C26H36N4P,C2H3N,Br
Inorganic chemistry (2016) 55, 14 7152-7166
a=10.3820(6)Å b=11.9178(7)Å c=13.2672(7)Å
α=73.322(2)° β=69.938(2)° γ=89.165(2)°
C22H40N4P,Br
C22H40N4P,Br
Inorganic chemistry (2016) 55, 14 7152-7166
a=12.3507(6)Å b=17.0313(8)Å c=12.0847(6)Å
α=90° β=100.871(2)° γ=90°
C18H21N4P,C2H3N,2(I)
C18H21N4P,C2H3N,2(I)
Inorganic chemistry (2016) 55, 14 7152-7166
a=9.6310(5)Å b=11.6495(7)Å c=21.6719(12)Å
α=90° β=102.066(2)° γ=90°
C14H24N4P,C2H3N,Br
C14H24N4P,C2H3N,Br
Inorganic chemistry (2016) 55, 14 7152-7166
a=6.9633(3)Å b=12.1035(5)Å c=22.8650(8)Å
α=90° β=98.1280(10)° γ=90°
C24H20B,C14H24AuClN4P,CH2Cl2
C24H20B,C14H24AuClN4P,CH2Cl2
Inorganic chemistry (2016) 55, 14 7152-7166
a=11.4611(5)Å b=13.1524(5)Å c=13.2357(6)Å
α=100.725(2)° β=93.311(2)° γ=92.065(2)°
(C18H32N4P),Br,0.33(C2H3N)
(C18H32N4P),Br,0.33(C2H3N)
Inorganic chemistry (2016) 55, 14 7152-7166
a=12.1188(9)Å b=12.1188(9)Å c=12.1188(9)Å
α=98.79° β=98.79° γ=98.79°
C18H20N4P,I
C18H20N4P,I
Inorganic chemistry (2016) 55, 14 7152-7166
a=16.6369(6)Å b=14.6559(6)Å c=16.2198(6)Å
α=90° β=106.4580(10)° γ=90°
C18H20PN4,CF3O3S
C18H20PN4,CF3O3S
Inorganic chemistry (2016) 55, 14 7152-7166
a=15.5193(3)Å b=15.7336(3)Å c=17.1506(3)Å
α=90° β=90° γ=90°
2(C14H24Au2Cl2N4P),3(C4H8O),2(AuCl2),CH2Cl2
2(C14H24Au2Cl2N4P),3(C4H8O),2(AuCl2),CH2Cl2
Inorganic chemistry (2016) 55, 14 7152-7166
a=25.2148(14)Å b=15.1025(9)Å c=16.1781(9)Å
α=90° β=95.4220(10)° γ=90°
C15H27N4P,2(CF3O3S)
C15H27N4P,2(CF3O3S)
Inorganic chemistry (2016) 55, 14 7152-7166
a=8.2808(6)Å b=14.1563(10)Å c=21.9892(17)Å
α=90° β=99.477(2)° γ=90°
C18H20N4PS2,I,C2H3N
C18H20N4PS2,I,C2H3N
Inorganic chemistry (2016) 55, 14 7152-7166
a=7.7142(4)Å b=17.3166(7)Å c=17.2570(8)Å
α=90° β=90° γ=90°
C14H24N4PS2,Br
C14H24N4PS2,Br
Inorganic chemistry (2016) 55, 14 7152-7166
a=20.7880(16)Å b=12.8659(7)Å c=14.3885(9)Å
α=90° β=90° γ=90°
C24H20B,C14H24N4P
C24H20B,C14H24N4P
Inorganic chemistry (2016) 55, 14 7152-7166
a=9.6887(8)Å b=29.759(3)Å c=11.3473(9)Å
α=90° β=92.616(2)° γ=90°
C14H24N4PH,2(CF3O3S)
C14H24N4PH,2(CF3O3S)
Inorganic chemistry (2016) 55, 14 7152-7166
a=8.8801(15)Å b=13.671(2)Å c=19.655(3)Å
α=90° β=97.227(3)° γ=90°
C18H20N4P,bR
C18H20N4P,bR
Inorganic chemistry (2016) 55, 14 7152-7166
a=20.0956(7)Å b=20.0956(7)Å c=18.3456(7)Å
α=90° β=90° γ=90°
C48H40AgBrN2P6
C48H40AgBrN2P6
Inorganic chemistry (2014) 141201074418004
a=20.9310(9)Å b=10.3138(4)Å c=12.3702(5)Å
α=90° β=124.1150(10)° γ=90°
C48H40BrCuN2P6,CH2Cl2,
C48H40BrCuN2P6,CH2Cl2,
Inorganic chemistry (2014) 141201074418004
a=21.2636(18)Å b=10.1246(7)Å c=15.1840(12)Å
α=90° β=133.915(5)° γ=90°
C58H46P6,0.81(C4H10O)
C58H46P6,0.81(C4H10O)
Inorganic chemistry (2014) 141201074418004
a=12.6149(11)Å b=13.2909(12)Å c=17.6210(16)Å
α=86.0290(10)° β=74.7350(10)° γ=83.9100(10)°
C24H56N2P8
C24H56N2P8
Inorganic chemistry (2014) 141201074418004
a=15.4287(13)Å b=13.3702(12)Å c=17.2421(15)Å
α=90° β=109.4820(10)° γ=90°
C48H40N2P6,CH2Cl2
C48H40N2P6,CH2Cl2
Inorganic chemistry (2014) 141201074418004
a=12.153(2)Å b=9.3574(16)Å c=20.114(3)Å
α=90° β=90.115(2)° γ=90°
C58H46P6
C58H46P6
Inorganic chemistry (2014) 141201074418004
a=8.8331(7)Å b=11.4721(10)Å c=12.3802(10)Å
α=74.9880(10)° β=72.7380(10)° γ=80.5270(10)°
C42H52Ag2Cl2N4
C42H52Ag2Cl2N4
Organometallics (2005) 24, 26 6301
a=21.0382(10)Å b=9.7005(5)Å c=9.9477(5)Å
α=90.00° β=90.00° γ=90.00°
C11H18AgClN2
C11H18AgClN2
Organometallics (2005) 24, 26 6301
a=8.1431(2)Å b=8.1431(2)Å c=20.5450(8)Å
α=90.00° β=90.00° γ=90.00°
C7H12AgClN2
C7H12AgClN2
Organometallics (2005) 24, 26 6301
a=10.5104(4)Å b=16.0633(6)Å c=11.2920(4)Å
α=90.00° β=100.5640(10)° γ=90.00°
C11H20AgClN2
C11H20AgClN2
Organometallics (2005) 24, 26 6301
a=19.1151(12)Å b=17.1519(11)Å c=17.3503(11)Å
α=90.00° β=97.1180(10)° γ=90.00°
C28H50AgCl3N2
C28H50AgCl3N2
Organometallics (2005) 24, 26 6301
a=16.1296(6)Å b=13.0986(5)Å c=16.5205(6)Å
α=90.00° β=116.7990(10)° γ=90.00°
C21H24AgClN2
C21H24AgClN2
Organometallics (2005) 24, 26 6301
a=17.0221(11)Å b=14.0448(9)Å c=17.2731(11)Å
α=90.00° β=90.00° γ=90.00°
C42H48Ag3I3N4
C42H48Ag3I3N4
Organometallics (2005) 24, 26 6301
a=11.8323(7)Å b=14.6993(8)Å c=15.6755(9)Å
α=65.5310(10)° β=69.4360(10)° γ=70.8040(10)°
C28.86H39.74AgCl4.74N2
C28.86H39.74AgCl4.74N2
Organometallics (2005) 24, 26 6301
a=9.7940(10)Å b=16.2939(16)Å c=10.9680(11)Å
α=90.00° β=103.488(2)° γ=90.00°
C29H42AgCl5N2
C29H42AgCl5N2
Organometallics (2005) 24, 26 6301
a=9.7788(15)Å b=16.334(3)Å c=21.755(3)Å
α=90.00° β=101.986(4)° γ=90.00°